Detection and determination of some pyrethroid pesticides in fruit and vegetable samples using Gas chromatography coupled to mass spectrometry

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KHANDAGHI J.; Afshar Mogaddam M.R.

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Paper Information

Journal: JOURNAL OF FOOD HYGIENE Year:2020 | Volume:10 | Issue:3 (39) Page(s): 1-13

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Title

Detection and determination of some pyrethroid pesticides in fruit and vegetable samples using Gas chromatography coupled to mass spectrometry

Author(s)

KHANDAGHI J. | Afshar Mogaddam M.R. | Issue Writer Certificate

Keywords

pyrethroid pesticidesQ1

homogeneous liquid-liquid microextractionQ1

gas chromatography coupled to mass spectrometryQ1

vegetableQ1

Abstract

The measurement of harmful substances that may enter the food has particular importance. Pesticides are one of the most important compounds that are wieldy used in agricultural activities. Despite the positive effects of the application of pesticides in agriculture, many pesticides are harmful to the environment and are known or suspected to be toxic to humans. pyrethroid pesticides are common pesticides used in agricultural and personal care products and due to their high efficiency in controlling different pests they are widely used. In the present work, an efficient and reliable microextraction method based on temperature-induced homogeneous liquid-liquid microextraction developed for the extraction of Delthamethrine, Biphenthrine, Permethrin, Cyhalothrin and Cypermethrine pyrethroid pesticides from potato, tomato, lettuce, and onion, and then its analyses performed using gas chromatography-mass spectrometry method. The optimized method was validated with recoveries ranging from 56 to 83%. The limits of detection were in the range of 4. 3-9. 4 ng mL-1, indicating high repeatability of the proposed method in the extraction and analysis of pyrethroid pesticides. Other advantages of this method include low cost and simplicity, low organic solvents consumption, and short analysis time.

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APA: Copy

KHANDAGHI, J., & Afshar Mogaddam, M.R.. (2020). Detection and determination of some pyrethroid pesticides in fruit and vegetable samples using Gas chromatography coupled to mass spectrometry. JOURNAL OF FOOD HYGIENE, 10(3 (39) ), 1-13. SID. https://sid.ir/paper/402336/en

Vancouver: Copy

KHANDAGHI J., Afshar Mogaddam M.R.. Detection and determination of some pyrethroid pesticides in fruit and vegetable samples using Gas chromatography coupled to mass spectrometry. JOURNAL OF FOOD HYGIENE[Internet]. 2020;10(3 (39) ):1-13. Available from: https://sid.ir/paper/402336/en

IEEE: Copy

J. KHANDAGHI, and M.R. Afshar Mogaddam, “Detection and determination of some pyrethroid pesticides in fruit and vegetable samples using Gas chromatography coupled to mass spectrometry,” JOURNAL OF FOOD HYGIENE, vol. 10, no. 3 (39) , pp. 1–13, 2020, [Online]. Available: https://sid.ir/paper/402336/en

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