DESIGN AND SYNTHESIS OF NEW SULFAMOYLACETAMIDE DERIVED FROM ANILINE UNDER SOLVENT FREE CONDITION

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MASSAH A.R.; ALAVI S.R.

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Seminar Paper

Paper Information

Seminar: IRANIAN SEMINAR OF ORGANIC CHEMISTRY
Year:2014 | Issue:22

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Title

DESIGN AND SYNTHESIS OF NEW SULFAMOYLACETAMIDE DERIVED FROM ANILINE UNDER SOLVENT FREE CONDITION

Author(s)

MASSAH A.R. | ALAVI S.R. | Issue Writer Certificate

Keywords

2-MERCAPTOBENZOTHIAZOLE

SULFAMOYLACETAMIDE

SOLVENT FREE

Abstract

SULFONAMIDES WERE INTENSIVELY INVESTIGATED AS THE FIRST EFFECTIVE ANTIBACTERIAL AGENTS. [1] DIFFERENT 2- (BENZO [D] THIAZOL-2-YLTHIO) -N - (4- (N-PHENYLSULFAMOYL) PHENYL) ACETAMIDE WERE SYNTHESIZED IN FOUR STEP, AS SHOWN IN SCHEME. FIRSTLY, ANILINE WAS ACYLATED WITH 2-CHLORO ACETYL CHLORIDE. THE PRODUCT (1) WAS REACTED WITH HSO3CL TO PRODUCE 4- (2-CHLOROACETAMIDO) BENZENE-1-SULFONYLCHLORIDE (2). DERIVATIVES OF COMPOUND (3) WAS SYNTHESIZED BY THE REACTION OF 2 WITH DIFFERENT AMINE. [2] IN THE FINAL STEP 2-MERCAPTO BENZOTHIAZOLE WAS REACTED WITH 2-CHLORO-N - (SULFAMOYL) ACETAMIDE. THE SULFONAMIDE WAS OBTAINED IN HIGH YIELD AND PURITY AFTER AN EASY WORK-UP.ANTIBACTERIAL ASSAY OF ALL THE TEST COMPOUNDS SHOWED GOOD ACTIVITIES AGAINST BOTH OF GRAM POSITIVE BACTERIA AND GRAM NEGATIVE BACTERIA.

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APA: Copy

MASSAH, A.R., & ALAVI, S.R.. (2014). DESIGN AND SYNTHESIS OF NEW SULFAMOYLACETAMIDE DERIVED FROM ANILINE UNDER SOLVENT FREE CONDITION. IRANIAN SEMINAR OF ORGANIC CHEMISTRY. SID. https://sid.ir/paper/914748/en

Vancouver: Copy

MASSAH A.R., ALAVI S.R.. DESIGN AND SYNTHESIS OF NEW SULFAMOYLACETAMIDE DERIVED FROM ANILINE UNDER SOLVENT FREE CONDITION. 2014. Available from: https://sid.ir/paper/914748/en

IEEE: Copy

A.R. MASSAH, and S.R. ALAVI, “DESIGN AND SYNTHESIS OF NEW SULFAMOYLACETAMIDE DERIVED FROM ANILINE UNDER SOLVENT FREE CONDITION,” presented at the IRANIAN SEMINAR OF ORGANIC CHEMISTRY. 2014, [Online]. Available: https://sid.ir/paper/914748/en

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