Impact of Pharmaceutical Impurities in Ecstasy Tablets: Gas Chromatography-Mass Spectrometry Study

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JALALI AMIR; HATAMIE AMIR; Saferpour Tahere; Khajeamiri Ali Reza; Safa Tahere; BUAZAR FOAD

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Journal Paper

Paper Information

Journal: Iranian Journal of Pharmaceutical Research Year:2016 | Volume:15 | Issue:1 Page(s): 221-229

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Title

Impact of Pharmaceutical Impurities in Ecstasy Tablets: Gas Chromatography-Mass Spectrometry Study

Author(s)

Keywords

Gas chromatography–

Mass Spectrometry (GC–

MS)

Identification

Determination

MDMA

Iran

Abstract

AbstractIn this study, a simple and reliable method by gas chromatograph– mass spectrometry (GC– MS) was developed for the fast and regular identification of 3, 4-MDMA impurities in ecstasy tablets. In so doing, 8 samples of impurities were extracted by diethyl ether under alkaline condition and then analyzed by GC– MS. The results revealed high MDMA levels ranging from 37. 6% to 57. 7%. The GC-MS method showed that unambiguous identification can be achieved for MDMA from 3, 4-methylenedioxyamphetamine (MDA), Amphetamine (AM), methamphetamine (MA) and ketamine (Keta) compounds, respectively. The experimental results indicated the acceptable time window without interfering peaks. It is found that GC-MS was provided a suitable and rapid identification approach for MDMA (Ecstacy) tablets, particularly in the Forensic labs. Consequently, the intense MDMA levels would support the police to develop a simple quantification of impurity in Ecstasy tablets.

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APA: Copy

JALALI, AMIR, HATAMIE, AMIR, Saferpour, Tahere, Khajeamiri, Ali Reza, Safa, Tahere, & BUAZAR, FOAD. (2016). Impact of Pharmaceutical Impurities in Ecstasy Tablets: Gas Chromatography-Mass Spectrometry Study. IRANIAN JOURNAL OF PHARMACEUTICAL RESEARCH (IJPR), 15(1), 221-229. SID. https://sid.ir/paper/288552/en

Vancouver: Copy

JALALI AMIR, HATAMIE AMIR, Saferpour Tahere, Khajeamiri Ali Reza, Safa Tahere, BUAZAR FOAD. Impact of Pharmaceutical Impurities in Ecstasy Tablets: Gas Chromatography-Mass Spectrometry Study. IRANIAN JOURNAL OF PHARMACEUTICAL RESEARCH (IJPR)[Internet]. 2016;15(1):221-229. Available from: https://sid.ir/paper/288552/en

IEEE: Copy

AMIR JALALI, AMIR HATAMIE, Tahere Saferpour, Ali Reza Khajeamiri, Tahere Safa, and FOAD BUAZAR, “Impact of Pharmaceutical Impurities in Ecstasy Tablets: Gas Chromatography-Mass Spectrometry Study,” IRANIAN JOURNAL OF PHARMACEUTICAL RESEARCH (IJPR), vol. 15, no. 1, pp. 221–229, 2016, [Online]. Available: https://sid.ir/paper/288552/en

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