HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC ANALYSIS OF ALMOTRIPTAN MALATE IN BULK AND TABLETS

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LAVUDU PETIKAM; PRAMEELA RANI AVULA; DIVYA CHEPURI; BALA SEKARAN CHANDRA

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Journal Paper

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Journal: Advanced Pharmaceutical Bulletin Year:2013 | Volume:3 | Issue:1 Page(s): 183-188

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Title

HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC ANALYSIS OF ALMOTRIPTAN MALATE IN BULK AND TABLETS

Author(s)

LAVUDU PETIKAM | PRAMEELA RANI AVULA | DIVYA CHEPURI | BALA SEKARAN CHANDRA | Issue Writer Certificate

Keywords

ALMOTRIPTAN MALATE

HPLC

VALIDATION

TABLETS

ANALYSIS

Abstract

Purpose: A simple RP-HPLC method has been developed and validated for the determination of ALMOTRIPTAN MALATE (ATM) in bulk and TABLETS.Methods: Chromatographic separation of ATM was achieved by using a Thermo Scientific C18 column. A Mobile phase containing a mixture of methanol, water and acetic acid (4: 8: 0.1 v/v) was pumped at the flow rate of 1 mL/min. Detection was performed at 227 nm. According to ICH guidelines, the method was validated.Results: The calibration curve was linear in the concentration range 5–60 mg/mL for the ATM with regression coefficient 0.9999. The method was precise with RSD<1.2%. Excellent recoveries of 99.60 - 100.80% proved the accuracy of the method. The limits of detection and quantification were found to be 0.025 and 0.075 mg/mL, respectively.Conclusion: The method was successfully applied for the quantification of ATM in TABLETS with acceptable accuracy and precision.

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APA: Copy

LAVUDU, PETIKAM, PRAMEELA RANI, AVULA, DIVYA, CHEPURI, & BALA SEKARAN, CHANDRA. (2013). HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC ANALYSIS OF ALMOTRIPTAN MALATE IN BULK AND TABLETS. ADVANCED PHARMACEUTICAL BULLETIN, 3(1), 183-188. SID. https://sid.ir/paper/331674/en

Vancouver: Copy

LAVUDU PETIKAM, PRAMEELA RANI AVULA, DIVYA CHEPURI, BALA SEKARAN CHANDRA. HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC ANALYSIS OF ALMOTRIPTAN MALATE IN BULK AND TABLETS. ADVANCED PHARMACEUTICAL BULLETIN[Internet]. 2013;3(1):183-188. Available from: https://sid.ir/paper/331674/en

IEEE: Copy

PETIKAM LAVUDU, AVULA PRAMEELA RANI, CHEPURI DIVYA, and CHANDRA BALA SEKARAN, “HIGH PERFORMANCE LIQUID CHROMATOGRAPHIC ANALYSIS OF ALMOTRIPTAN MALATE IN BULK AND TABLETS,” ADVANCED PHARMACEUTICAL BULLETIN, vol. 3, no. 1, pp. 183–188, 2013, [Online]. Available: https://sid.ir/paper/331674/en

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