SURVEY OF AMITRAZ RESIDUE IN SOME HONEY SAMPLES BY MICROEXTRACTION METHOD AND OPTIMIZATION USING AN EXPERIMENTAL DESIGN

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FARAJI M.; AMINI KADIJANI P.

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Paper Information

Journal: IRANIAN JOURNAL OF NUTRITION SCIENCES AND FOOD TECHNOLOGY Year:2015 | Volume:10 | Issue:2 Page(s): 67-76

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Title

SURVEY OF AMITRAZ RESIDUE IN SOME HONEY SAMPLES BY MICROEXTRACTION METHOD AND OPTIMIZATION USING AN EXPERIMENTAL DESIGN

Author(s)

FARAJI M. | AMINI KADIJANI P. | Issue Writer Certificate

Keywords

AMITRAZQ2

HOLLOW FIBER LIQUID PHASE MICROEXTRACTIONQ2

ORTHOGONAL ARRAY DESIGNQ2

HONEY SAMPLEQ2

Abstract

Background and Objectives: Amitraz is an insecticide and pesticide that, due to exceptionally strong parasiticide activities, is widely used for biological pollution monitoring. The purpose of this research was to develop and validate a liquid phase extraction technique with hollow fibers (HF-LPME) in order to determine amitraz residue in honey samples.Materials and Methods: Method of Hollow fiber liquid phase microextraction (HF-LPME) was used as simple, fast, low cost and sensitive method for determination of the amitraz from honey samples by gas chromatography flame ionization detection. Effects of five experimental factors: type of the extracting solvent, pH of the sample, stirring rate, extraction time and percent of NaCl were studied and optimized.Results: Analysis of variance showed that percent of salt and stirring rate have major effect on the extraction of amitraz (p=0.05). Method in honey matrix was linear in the range from 20 to 1000 ng/mL with RSD lower than 14% and r2>0.9901. Enrichment factor was 75; also the limit of detection (LOD) based on S/N=3 was 10 ng/mL.Conclusion: According to obtained high recovery (>90%) of Amitraz by applying HF-LPME method in honey samples, this method is suggested as simple, rapid and sensitive technique.

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References

APPLICATION OF HOLLOW FIBER SUPPORTED LIQUID MEMBRANE EXTRACTION TO THE SIMULTANEOUS DETERMINATION OF PESTICIDE RESIDUES IN VEGETABLES BY LIQUID CHROMATOGRAPHY/MASS SPECTROMETRY

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APA: Copy

FARAJI, M., & AMINI KADIJANI, P.. (2015). SURVEY OF AMITRAZ RESIDUE IN SOME HONEY SAMPLES BY MICROEXTRACTION METHOD AND OPTIMIZATION USING AN EXPERIMENTAL DESIGN. JOURNAL OF NUTRITION SCIENCES & FOOD TECHNOLOGY, 10(2), 67-76. SID. https://sid.ir/paper/121354/en

Vancouver: Copy

FARAJI M., AMINI KADIJANI P.. SURVEY OF AMITRAZ RESIDUE IN SOME HONEY SAMPLES BY MICROEXTRACTION METHOD AND OPTIMIZATION USING AN EXPERIMENTAL DESIGN. JOURNAL OF NUTRITION SCIENCES & FOOD TECHNOLOGY[Internet]. 2015;10(2):67-76. Available from: https://sid.ir/paper/121354/en

IEEE: Copy

M. FARAJI, and P. AMINI KADIJANI, “SURVEY OF AMITRAZ RESIDUE IN SOME HONEY SAMPLES BY MICROEXTRACTION METHOD AND OPTIMIZATION USING AN EXPERIMENTAL DESIGN,” JOURNAL OF NUTRITION SCIENCES & FOOD TECHNOLOGY, vol. 10, no. 2, pp. 67–76, 2015, [Online]. Available: https://sid.ir/paper/121354/en

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